Design of a scanning tunneling microscope for electrochemical applications

Moris M. Dovek, Michael J. Heben, Christoph A. Lang, Nathan S Lewis, Calvin F. Quate

Research output: Contribution to journalArticle

17 Citations (Scopus)

Abstract

A design for a scanning tunneling microscope that is well suited for electrochemical investigations is presented. The construction of the microscope ensures that only the tunneling tip and the sample participate in electrochemical reactions. The design also allows rapid replacement of the tip or sample, and enables facile introduction of auxiliary electrodes for use in electrochemical experiments. The microscope utilizes stepper motor driven approach mechanics in order to achieve fully remote operation and to allow reproducible coarse control of tip/sample spacings for electrochemical experiments. Highly ordered pyrolytic graphite images at atomic resolution in air and aqueous solutions can be obtained with this microscope.

Original languageEnglish
Pages (from-to)2333-2336
Number of pages4
JournalReview of Scientific Instruments
Volume59
Issue number11
DOIs
Publication statusPublished - 1988

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Microscopes
microscopes
Scanning
scanning
pyrolytic graphite
Mechanics
Graphite
Experiments
spacing
aqueous solutions
Electrodes
electrodes
air
Air

ASJC Scopus subject areas

  • Instrumentation
  • Physics and Astronomy (miscellaneous)

Cite this

Design of a scanning tunneling microscope for electrochemical applications. / Dovek, Moris M.; Heben, Michael J.; Lang, Christoph A.; Lewis, Nathan S; Quate, Calvin F.

In: Review of Scientific Instruments, Vol. 59, No. 11, 1988, p. 2333-2336.

Research output: Contribution to journalArticle

Dovek, Moris M. ; Heben, Michael J. ; Lang, Christoph A. ; Lewis, Nathan S ; Quate, Calvin F. / Design of a scanning tunneling microscope for electrochemical applications. In: Review of Scientific Instruments. 1988 ; Vol. 59, No. 11. pp. 2333-2336.
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