Abstract
ZnO solidus and liquidus boundaries in the ZnO-Bi2O3 system were investigated via analytical electron microscopy (AEM), electron probe microanalysis (EPMA), and secondary ion mass spectrometry (SIMS). The Bi2O3 solubility is highest - 0.24 ± 0.04 mol% - at the eutectic temperature of 740°C and decreases rapidly with increasing temperature. Detection limits and quantification procedures of X-ray microanalysis (AEM, EPMA) and ion microanalysis (SIMS) are discussed with respect to the determination of phase diagrams involving low solubility phases.
| Original language | English |
|---|---|
| Pages (from-to) | 1499-1504 |
| Number of pages | 6 |
| Journal | Journal of the American Ceramic Society |
| Volume | 77 |
| Issue number | 6 |
| Publication status | Published - Jun 1994 |
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ASJC Scopus subject areas
- Ceramics and Composites
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Microanalytical determination of ZnO solidus and liquidus boundaries in the ZnO-Bi2O3 system. / Hwang, Jin Ha; Mason, Thomas O; Dravid, Vinayak P.
In: Journal of the American Ceramic Society, Vol. 77, No. 6, 06.1994, p. 1499-1504.Research output: Contribution to journal › Article
}
TY - JOUR
T1 - Microanalytical determination of ZnO solidus and liquidus boundaries in the ZnO-Bi2O3 system
AU - Hwang, Jin Ha
AU - Mason, Thomas O
AU - Dravid, Vinayak P.
PY - 1994/6
Y1 - 1994/6
N2 - ZnO solidus and liquidus boundaries in the ZnO-Bi2O3 system were investigated via analytical electron microscopy (AEM), electron probe microanalysis (EPMA), and secondary ion mass spectrometry (SIMS). The Bi2O3 solubility is highest - 0.24 ± 0.04 mol% - at the eutectic temperature of 740°C and decreases rapidly with increasing temperature. Detection limits and quantification procedures of X-ray microanalysis (AEM, EPMA) and ion microanalysis (SIMS) are discussed with respect to the determination of phase diagrams involving low solubility phases.
AB - ZnO solidus and liquidus boundaries in the ZnO-Bi2O3 system were investigated via analytical electron microscopy (AEM), electron probe microanalysis (EPMA), and secondary ion mass spectrometry (SIMS). The Bi2O3 solubility is highest - 0.24 ± 0.04 mol% - at the eutectic temperature of 740°C and decreases rapidly with increasing temperature. Detection limits and quantification procedures of X-ray microanalysis (AEM, EPMA) and ion microanalysis (SIMS) are discussed with respect to the determination of phase diagrams involving low solubility phases.
UR - http://www.scopus.com/inward/record.url?scp=0028459805&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=0028459805&partnerID=8YFLogxK
M3 - Article
VL - 77
SP - 1499
EP - 1504
JO - Journal of the American Ceramic Society
JF - Journal of the American Ceramic Society
SN - 0002-7820
IS - 6
ER -