Abstract
A wide range of ultra-fine, nano-crystalline powders and suspensions havebeen produced using the Rapid Thermal Decomposition of precursors in Solution (RTDS) technology. These materials include single and multi-component iron-, zirconium-, titanium-, nickel-, and chromium-oxide/oxyhydroxide powders. RTDS, which was developed at Pacific Northwest Laboratory, is a flow-through hydrothermal process capable of producing nano-crystalline particulate material at rates of up to 100 grams of solid per hour. We present the results of characterization efforts on RTDS iron oxyhydroxide and zirconium oxide systems. As-collected RTDS suspensions were characterized using optical light scattering. Separated RTDS powders were evaluated using X-ray diffraction, electron microscopy, gas adsorption analysis, thermal gravimetric analysis, and chemical analysis.
| Original language | English |
|---|---|
| Title of host publication | Materials Research Society Symposium - Proceedings |
| Publisher | Materials Research Society |
| Pages | 499-504 |
| Number of pages | 6 |
| Volume | 346 |
| Publication status | Published - 1994 |
| Event | Proceedings of the 1994 MRS Spring Meeting - San Francisco, CA, USA Duration: Apr 4 1994 → Apr 8 1994 |
Other
| Other | Proceedings of the 1994 MRS Spring Meeting |
|---|---|
| City | San Francisco, CA, USA |
| Period | 4/4/94 → 4/8/94 |
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ASJC Scopus subject areas
- Electronic, Optical and Magnetic Materials
Cite this
Nano-crystalline powders and suspensions generated using a flow-through hydrothermal process, part I : Characterization. / Darab, John G.; Buehler, M. F.; Linehan, John; Matson, D. W.
Materials Research Society Symposium - Proceedings. Vol. 346 Materials Research Society, 1994. p. 499-504.Research output: Chapter in Book/Report/Conference proceeding › Conference contribution
}
TY - GEN
T1 - Nano-crystalline powders and suspensions generated using a flow-through hydrothermal process, part I
T2 - Characterization
AU - Darab, John G.
AU - Buehler, M. F.
AU - Linehan, John
AU - Matson, D. W.
PY - 1994
Y1 - 1994
N2 - A wide range of ultra-fine, nano-crystalline powders and suspensions havebeen produced using the Rapid Thermal Decomposition of precursors in Solution (RTDS) technology. These materials include single and multi-component iron-, zirconium-, titanium-, nickel-, and chromium-oxide/oxyhydroxide powders. RTDS, which was developed at Pacific Northwest Laboratory, is a flow-through hydrothermal process capable of producing nano-crystalline particulate material at rates of up to 100 grams of solid per hour. We present the results of characterization efforts on RTDS iron oxyhydroxide and zirconium oxide systems. As-collected RTDS suspensions were characterized using optical light scattering. Separated RTDS powders were evaluated using X-ray diffraction, electron microscopy, gas adsorption analysis, thermal gravimetric analysis, and chemical analysis.
AB - A wide range of ultra-fine, nano-crystalline powders and suspensions havebeen produced using the Rapid Thermal Decomposition of precursors in Solution (RTDS) technology. These materials include single and multi-component iron-, zirconium-, titanium-, nickel-, and chromium-oxide/oxyhydroxide powders. RTDS, which was developed at Pacific Northwest Laboratory, is a flow-through hydrothermal process capable of producing nano-crystalline particulate material at rates of up to 100 grams of solid per hour. We present the results of characterization efforts on RTDS iron oxyhydroxide and zirconium oxide systems. As-collected RTDS suspensions were characterized using optical light scattering. Separated RTDS powders were evaluated using X-ray diffraction, electron microscopy, gas adsorption analysis, thermal gravimetric analysis, and chemical analysis.
UR - http://www.scopus.com/inward/record.url?scp=0028592408&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=0028592408&partnerID=8YFLogxK
M3 - Conference contribution
AN - SCOPUS:0028592408
VL - 346
SP - 499
EP - 504
BT - Materials Research Society Symposium - Proceedings
PB - Materials Research Society
ER -