TY - JOUR
T1 - Synthesis and structure of Nb3SiTe6, a new layered ternary niobium telluride compound
AU - Li, Jing
AU - Badding, Michael E.
AU - DiSalvo, F. J.
N1 - Funding Information:
We are grateful to the US Department of Energy, Division of Basic Energy Sciences, for its generous support through Grant DE-FG02-87ER45298. J.L. is grateful for a Research Council grant and the HeIuT Rutgers Research Fellowship in completion of this work.
PY - 1992/6/12
Y1 - 1992/6/12
N2 - Nb3SiTe6, a new type of layered ternary telluride compound, has been synthesized. The structure is determined by single-crystal X-ray diffraction methods. The compound crystallizes in space group Pnma (No. 62) with Z=4, a=6.353(2) A ̊, b=13.938(5) A ̊, c=11.507(4) A ̊, V=1018.9(6) A ̊3, R=4.77% and Rw=4.88%. The structure contains sheets of mixed niobium and silicon with tellurium atoms capping both sides. The layered framework has an unusual coordination environment.
AB - Nb3SiTe6, a new type of layered ternary telluride compound, has been synthesized. The structure is determined by single-crystal X-ray diffraction methods. The compound crystallizes in space group Pnma (No. 62) with Z=4, a=6.353(2) A ̊, b=13.938(5) A ̊, c=11.507(4) A ̊, V=1018.9(6) A ̊3, R=4.77% and Rw=4.88%. The structure contains sheets of mixed niobium and silicon with tellurium atoms capping both sides. The layered framework has an unusual coordination environment.
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U2 - 10.1016/0925-8388(92)90499-Y
DO - 10.1016/0925-8388(92)90499-Y
M3 - Article
AN - SCOPUS:0026873973
VL - 184
SP - 257
EP - 263
JO - Journal of Alloys and Compounds
JF - Journal of Alloys and Compounds
SN - 0925-8388
IS - 2
ER -